formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester

Base Information

Chemical Name:formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester
CAS No.:218461-44-0
Molecular Formula:C₁₉H₂₇NO₄
Molecular Weight:333.428
Hs Code.:

Synonyms:formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester

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Chemical Property of formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester

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Technology Process of formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester

There total 4 articles about formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 218461-34-8
1-(3-pentamethylphenylmethoxy-propyl)-4-vinyloxy-azetidin-2-one

: 218461-44-0
formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester

Guidance literature:: With dimethylsulfide; N-ethyl-1-[{4-(phenylazo)-phenyl}-azo]-2-naphthalenylamine; ozone; In dichloromethane; at -78 ℃;
DOI:10.1016/S0040-4039(98)01841-3

Reference yield:

: 484-65-1
2,3,4,5,6-pentamethylbenzyl chloride

: 218461-44-0
formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / dimethylformamide

2: 2,6-lutidine / CH₂Cl₂

3: Bu₄NHSO₄, butyllithium / tetrahydrofuran / -78 °C

4: O₃, dimethyl sulfide, Sudan red 7B / CH₂Cl₂ / -78 °C

With 2,6-dimethylpyridine; n-butyllithium; dimethylsulfide; N-ethyl-1-[{4-(phenylazo)-phenyl}-azo]-2-naphthalenylamine; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; ozone; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(98)01841-3

Reference yield:

: 218461-30-4
3-pentamethylphenylmethoxy-propan-1-ol

: 218461-44-0
formic acid 4-oxo-1-(3-pentamethylphenylmethoxy-propyl)-azetidin-2-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-lutidine / CH₂Cl₂

2: Bu₄NHSO₄, butyllithium / tetrahydrofuran / -78 °C

3: O₃, dimethyl sulfide, Sudan red 7B / CH₂Cl₂ / -78 °C

With 2,6-dimethylpyridine; n-butyllithium; dimethylsulfide; N-ethyl-1-[{4-(phenylazo)-phenyl}-azo]-2-naphthalenylamine; tetra(n-butyl)ammonium hydrogensulfate; ozone; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(98)01841-3