(2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)

Base Information

Chemical Name:(2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)
CAS No.:1262993-77-0
Molecular Formula:C₄₆H₅₆Br₄N₆O₆
Molecular Weight:1108.6
Hs Code.:

Synonyms:(2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)

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Technology Process of (2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)

There total 5 articles about (2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 61345-87-7
N,N <(amino-3 propyl) methyl> N',N'<(amino-3 propyl) methyl> butane diamine-1,4

: 1262993-75-8
C₁₇H₁₄Br₂ClNO₃

: 1262993-77-0
(2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)

Guidance literature:: With 2,6-dimethylpyridine; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2010.10.164

Reference yield: 62.0%

: 61345-87-7
N,N <(amino-3 propyl) methyl> N',N'<(amino-3 propyl) methyl> butane diamine-1,4

: 2-[benzyloxyimino]-3-(3, 5-dibromo-4-methoxy-phenyl)-propionic acid

: 1262993-77-0
(2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol303057a

Reference yield:

: 108940-96-1
3,5-dibromo-4-methoxybenzaldehyde

: 1262993-77-0
(2E,2'E)-N,N'-(3,3'-(butane-1,4-diylbis(methylazanediyl))bis(propane-3,1-diyl))bis(2-(benzyloxyimino)-3-(3,5-dibromo-4-methoxyphenyl)propanamide)

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / acetic acid / 110 - 120 °C / Inert atmosphere

2: sodium hydroxide / water / 80 - 90 °C / Inert atmosphere

3: sodium ethanolate / ethanol / 70 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C / Inert atmosphere

With sodium ethanolate; sodium acetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; acetic acid;
DOI:10.1021/ol303057a