Technology Process of C24H32O5
There total 7 articles about C24H32O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
perchloric acid;
In
dimethyl sulfoxide;
at 80 ℃;
for 5h;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 45 percent / (-)-diisopropyl tartrate; Ti(Oi-Pr)4; tert-butyl hydroperoxide / CH2Cl2; decane
2: 50 percent / BF3*Et2O / CH2Cl2 / 15 h / 20 °C
3: 81 percent / potassium carbonate / methanol / 1 h / 20 °C
4: 95 percent / aq. HClO4 / dimethylsulfoxide / 5 h / 80 °C
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; perchloric acid; (-)-diisopropyl tartrate; boron trifluoride diethyl etherate; potassium carbonate;
In
methanol; decane; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ol0701013
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 50 percent / BF3*Et2O / CH2Cl2 / 15 h / 20 °C
2: 81 percent / potassium carbonate / methanol / 1 h / 20 °C
3: 95 percent / aq. HClO4 / dimethylsulfoxide / 5 h / 80 °C
With
perchloric acid; boron trifluoride diethyl etherate; potassium carbonate;
In
methanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ol0701013