C₂₄H₂₁⁽²⁾HN₂O₇

Base Information

• Chemical Name: C₂₄H₂₁⁽²⁾HN₂O₇
• CAS No.: 148504-69-2
• Molecular Formula: C₂₄H₂₂N₂O₇
• Molecular Weight: 451.44
• Mol file: 148504-69-2.mol

Synonyms:C₂₄H₂₁⁽²⁾HN₂O₇

Chemical Property of C₂₄H₂₁⁽²⁾HN₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₂₄H₂₁⁽²⁾HN₂O₇

There total 3 articles about C₂₄H₂₁⁽²⁾HN₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-methyluridine (182004-59-7) → C24H21(2)HN2O7 (148504-69-2)

Guidance literature:

With d8-isopropanol; 9-ethyl-3,6-dimethoxy-9H-carbazole; In water; at 45 ℃; for 0.416667h; under 1034.32 Torr; Solvent; UV-irradiation;

DOI:10.1071/CH12426

Reference yield:

α-D-1,3,5-tri-O-benzoyl-2-O-[3-(trifluoromethyl)benzoyl]ribofuranose (145828-13-3) → C24H21(2)HN2O7 (148504-69-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,6-di-tert-butyl-4-methylpyridinium trifluoromethanesulfonate / acetonitrile / 0.5 h / 150 °C / 5171.62 Torr

2: 9-ethyl-3,6-dimethoxy-9H-carbazole; d8-isopropanol / water / 0.42 h / 45 °C / 1034.32 Torr / UV-irradiation

With d8-isopropanol; 9-ethyl-3,6-dimethoxy-9H-carbazole; 2,6-di-tert-butyl-4-methylpyridinium trifluoromethanesulfonate; In water; acetonitrile;

DOI:10.1071/CH12426

Reference yield:

5-methyl-2,4-bis-trimethylsilanyloxy-pyridine (50503-53-2) → C24H21(2)HN2O7 (148504-69-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 2,6-di-tert-butyl-4-methylpyridinium trifluoromethanesulfonate / acetonitrile / 0.5 h / 150 °C / 5171.62 Torr

2: 9-ethyl-3,6-dimethoxy-9H-carbazole; d8-isopropanol / water / 0.42 h / 45 °C / 1034.32 Torr / UV-irradiation

With d8-isopropanol; 9-ethyl-3,6-dimethoxy-9H-carbazole; 2,6-di-tert-butyl-4-methylpyridinium trifluoromethanesulfonate; In water; acetonitrile;

DOI:10.1071/CH12426

upstream raw materials:

3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-methyluridine

α-D-1,3,5-tri-O-benzoyl-2-O-[3-(trifluoromethyl)benzoyl]ribofuranose

5-methyl-2,4-bis-trimethylsilanyloxy-pyridine