(4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

Base Information

Chemical Name:(4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol
CAS No.:207224-05-3
Molecular Formula:C₄₀H₅₈O₇
Molecular Weight:650.896
Hs Code.:

(4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

Synonyms:(4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

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Chemical Property of (4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

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Technology Process of (4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

There total 10 articles about (4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 207224-04-2
C₄₂H₆₂O₈

: 207224-05-3
(4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

Guidance literature:: With lithium tetrafluoroborate; In water; acetonitrile; at 70 ℃; for 49h;
DOI:10.1002/hlca.19980810313

Reference yield:

: 146952-73-0
[4-({[tert-butyl(diphenyl)silyl]oxy}methyl)phenyl]methanol

: 207224-05-3
(4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

Guidance literature:: Multi-step reaction with 5 steps

1: Ph₃P, Br₂ / tetrahydrofuran / 13 h / Ambient temperature

2: 1) BuLi (1.5M in hexane, (iPr)2NH / 1) THF, 0 deg C, 15 min, 2) THF, -78 deg C, 30 h

3: 92 percent / NaBH₄ / tetrahydrofuran; methanol / 0 deg C, 2 h; RT, 14.5 h

4: 1) NaH / 1) THF, 0 deg C, 15 min then RT, 15 min and 70 deg C, 30 min, 2) THF, RT, 1.5 h then reflux, 1 h and RT, 20 h, then reflux, 4 h

5: Bu₄NF / tetrahydrofuran / 24 h / Ambient temperature

With sodium tetrahydroborate; n-butyllithium; tetrabutyl ammonium fluoride; bromine; sodium hydride; diisopropylamine; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.19980810313

Reference yield:

: 207223-99-2
1-Bromomethyl-4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzene

: 207224-05-3
(4-{(2S,3R)-3-[4-((2S,3R)-3-Methoxy-2-methoxymethyl-butyl)-benzyloxy]-2-[4-((2S,3R)-3-methoxy-2-methoxymethyl-butyl)-benzyloxymethyl]-butyl}-phenyl)-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) THF, 0 deg C, 15 min then RT, 15 min and 70 deg C, 30 min, 2) THF, RT, 1.5 h then reflux, 1 h and RT, 20 h, then reflux, 4 h

2: Bu₄NF / tetrahydrofuran / 24 h / Ambient temperature

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran;
DOI:10.1002/hlca.19980810313