Technology Process of C23H22BrNO
There total 4 articles about C23H22BrNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H16BrNO;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
at 0 - 20 ℃;
benzyl bromide;
In
tetrahydrofuran; mineral oil;
at 0 - 20 ℃;
DOI:10.1021/ol200149s
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 0 °C
2.1: thionyl chloride / 2 h / Reflux
3.1: triethylamine / dichloromethane / 0 - 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C
4.2: 0 - 20 °C
With
thionyl chloride; sodium hydride; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol200149s
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: thionyl chloride / 2 h / Reflux
2.1: triethylamine / dichloromethane / 0 - 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C
3.2: 0 - 20 °C
With
thionyl chloride; sodium hydride; triethylamine;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol200149s