4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide

Base Information

Chemical Name:4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide
CAS No.:58914-41-3
Molecular Formula:C₂₈H₃₁N₃O₅
Molecular Weight:489.571
Hs Code.:

Synonyms:4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide

There total 3 articles about 4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18969-60-3
4-[(2-methyl-1,2-dicarbobenzoxy-hydrazino)-methyl]-benzoic acid

: 75-31-0
isopropylamine

: 58914-41-3
4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide

Guidance literature:: In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dichloromethane; benzene;

Reference yield:

: 99-75-2
4-methyl-benzoic acid methyl ester

: 58914-41-3
4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / Irradiation

2: (i) NaH, DMF, (ii) aq. NaOH

3: (i) SOCl₂, (ii) /BRN= 605259/, benzene

With bromine;

Reference yield:

: 6002-83-1
1-methyl-1,2-dicarbobenzoxy-hydrazine

: 58914-41-3
4-[(2-methyl-1,2-dicarbobenzoxyhydrazino)-methyl]-benzoic acid isopropylamide

Guidance literature:: Multi-step reaction with 2 steps

1: (i) NaH, DMF, (ii) /BRN= 1867272/, (iii) aq. NaOH, dioxane

2: (i) SOCl₂, (ii) /BRN= 605259/, benzene