2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

Base Information

Chemical Name:2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide
CAS No.:1033617-40-1
Molecular Formula:C₂₀H₃₇NO₂SSi₂
Molecular Weight:411.756
Hs Code.:

Synonyms:2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

Suppliers and Price of 2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

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Technology Process of 2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

There total 1 articles about 2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1033617-39-8
2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)acetamide

: 1033617-40-1
2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

Guidance literature:: With Lawessons reagent; In toluene; at 70 ℃; for 2h;
DOI:10.1016/j.bmc.2008.02.035

Reference yield: 89.0%

: 41355-50-4,51642-81-0,58484-22-3,70128-27-7,70145-20-9,94482-21-0,98300-76-6
2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine

: 1033617-40-1
2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

: 1033617-41-2
N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine

Guidance literature:: 2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide; With trimethoxonium tetrafluoroborate; In dichloromethane; at 20 ℃; for 14h;

2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine; With 4 A molecular sieve; In dichloromethane; for 0.25h;

With N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 2h; Further stages.;
DOI:10.1016/j.bmc.2008.02.035