N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine

Base Information

Chemical Name:N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine
CAS No.:1033617-41-2
Molecular Formula:C₃₄H₅₆N₂O₁₁Si₂
Molecular Weight:724.996
Hs Code.:

Synonyms:N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine

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Technology Process of N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine

There total 1 articles about N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 41355-50-4,51642-81-0,58484-22-3,70128-27-7,70145-20-9,94482-21-0,98300-76-6
2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine

: 1033617-40-1
2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide

: 1033617-41-2
N-(p-(tert-butyldimethylsilyloxy)phenyl)-N'-(2,3,4,6-tetraacetyl-1-β-D-glucopyranosyl)-(tert-butyldimethylsilyloxy)methylamidine

Guidance literature:: 2-(tert-butyldimethylsilyloxy)-N-(p-(tert-butyldimethylsilyloxy)phenyl)thioacetamide; With trimethoxonium tetrafluoroborate; In dichloromethane; at 20 ℃; for 14h;

2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine; With 4 A molecular sieve; In dichloromethane; for 0.25h;

With N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 2h; Further stages.;
DOI:10.1016/j.bmc.2008.02.035