4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester

Base Information

Chemical Name:4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester
CAS No.:172976-57-7
Molecular Formula:C₂₆H₁₃BrClF₅O₂
Molecular Weight:567.737
Hs Code.:

Synonyms:4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester

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Chemical Property of 4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester

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Technology Process of 4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester

There total 4 articles about 4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 172976-56-6
2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

: 172976-57-7
4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester

Guidance literature:: With Acetyl bromide; In dichloromethane; for 1.25h; Ambient temperature;
DOI:10.1021/ja00152a005

Reference yield:

: 5162-03-8
(2-chlorophenyl)(phenyl)methanone

: 172976-57-7
4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, from -78 deg C to RT, 1 h

2: 80.3 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 3 h

3: acetyl bromide / CH₂Cl₂ / 1.25 h / Ambient temperature

With n-butyllithium; Acetyl bromide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00152a005

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 172976-57-7
4-[Bromo-(2-chloro-phenyl)-phenyl-methyl]-benzoic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, from -78 deg C to RT, 1 h

2: 80.3 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 3 h

3: acetyl bromide / CH₂Cl₂ / 1.25 h / Ambient temperature

With n-butyllithium; Acetyl bromide; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00152a005