2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

Base Information

Chemical Name:2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester
CAS No.:172976-56-6
Molecular Formula:C₂₆H₁₄ClF₅O₃
Molecular Weight:504.84
Hs Code.:

Synonyms:2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

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Chemical Property of 2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

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Technology Process of 2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

There total 3 articles about 2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.3%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 172976-68-0
(R,S) 2-chloro-4'-carboxy-triphenyl methanol

: 172976-56-6
2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; for 3h;
DOI:10.1021/ja00152a005

Reference yield:

: 5162-03-8
(2-chlorophenyl)(phenyl)methanone

: 172976-56-6
2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, from -78 deg C to RT, 1 h

2: 80.3 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 3 h

With n-butyllithium; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/ja00152a005

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 172976-56-6
2-chloro-4'-carboxytriphenylmethanol pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) THF, hexane, -78 deg C, 45 min, 2.) THF, hexane, from -78 deg C to RT, 1 h

2: 80.3 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 3 h

With n-butyllithium; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/ja00152a005