(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

Base Information

Chemical Name:(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate
CAS No.:1420376-74-4
Molecular Formula:C₂₈H₄₁O₅P
Molecular Weight:488.604
Hs Code.:

Synonyms:(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

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Chemical Property of (1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

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Technology Process of (1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

There total 1 articles about (1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1420376-56-2
2-(diethoxy-phosphoryl)-acrylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 1420376-74-4
(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -65 ℃; for 12h; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.11.021

Reference yield: 52.0%

: 1420376-74-4
(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

: 99-33-2
3,5-dinitrobenoyl chloride

: 1420376-95-9
3,5-dinitro-benzoic acid 2-(diethoxy-phosphoryl)-bicyclo[2.2.1]hept-5-en-2-ylmethyl ester

Guidance literature:: (1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate; With diisobutylaluminium hydride; In toluene; at -78 - 20 ℃; Inert atmosphere;

3,5-dinitrobenoyl chloride; With pyridine; dmap; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.11.021

Reference yield: 47.0%

: 1420376-74-4
(1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

: 74-88-4
methyl iodide

: 1420377-01-0
C₂₅H₃₄O₂

: 4-(1R,2S,5R,3'R,4'R,6'R)-[5-methyl-2-(1-methyl-1-phenylethyl)-cyclohexyloxycarbonyl]-4-methylbicyclo[2.2.1]heptene

Guidance literature:: (1R,2S,5R)-5-methyl-2-(2-phenylpropan-2-yl)cyclohexyl (1R,2S,4R)-2-(diethoxyphosphoryl)bicyclo[2.2.1]hept-5-ene-2-carboxylate; With naphthalen-1-yl-lithium; In tetrahydrofuran; at -60 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at -20 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tetasy.2012.11.021