C₂₉H₄₄O₂Si

Base Information

Chemical Name:C₂₉H₄₄O₂Si
CAS No.:943898-23-5
Molecular Formula:C₂₉H₄₄O₂Si
Molecular Weight:452.753
Hs Code.:

C<sub>29</sub>H<sub>44</sub>O<sub>2</sub>Si

Synonyms:C₂₉H₄₄O₂Si

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Chemical Property of C₂₉H₄₄O₂Si

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Technology Process of C₂₉H₄₄O₂Si

There total 8 articles about C₂₉H₄₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 943898-01-9
C₂₉H₄₆O₂Si

: 943898-23-5
C₂₉H₄₄O₂Si

Guidance literature:: With N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; In dichloromethane; at 20 ℃;
DOI:10.1021/ol070517g

Reference yield:

: 633323-32-7
C₂₉H₄₄SiO₃

: 943898-23-5
C₂₉H₄₄O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 90 percent / lithium hydroxide monohydrate / tetrahydrofuran; methanol; H₂O / 5 h / 20 °C

2.1: oxalyl chloride / benzene; dimethylformamide / 4 h / 20 °C

3.1: 92 percent / butyllithium / tetrahydrofuran; hexane / -78 °C

4.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / -78 °C

4.2: 78 percent / tetrahydrofuran / 5 h / -78 °C

5.1: 90 percent / lithium borohydride / diethyl ether; ethanol / 2 h / 0 °C

6.1: 82 percent / activated molecular sieves 4 Angstroem; NMO; TPAP / CH₂Cl₂ / 20 °C

With lithium hydroxide; lithium borohydride; n-butyllithium; N-methyl-2-indolinone; tetrapropylammonium perruthennate; oxalyl dichloride; 4 A molecular sieve; sodium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ol070517g

Reference yield:

: 943897-99-2
C₃₈H₅₁O₄SiN

: 943898-23-5
C₂₉H₄₄O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 78 percent / tetrahydrofuran / 5 h / -78 °C

2.1: 90 percent / lithium borohydride / diethyl ether; ethanol / 2 h / 0 °C

3.1: 82 percent / activated molecular sieves 4 Angstroem; NMO; TPAP / CH₂Cl₂ / 20 °C

With lithium borohydride; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; sodium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/ol070517g