methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt

Base Information

Chemical Name:methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt
CAS No.:1346551-15-2
Molecular Formula:C₁₁H₁₅NO₅P*Na
Molecular Weight:295.207
Hs Code.:

Synonyms:methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt

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Chemical Property of methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt

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Technology Process of methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt

There total 3 articles about methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82629-22-9
1-(N-benzyloxycarbonylamino)ethylphosphonic acid dimethyl ester

: 1346551-15-2
methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt

Guidance literature:: With sodium iodide; In acetone; for 0.0833333h; Reflux;
DOI:10.1016/j.bmcl.2011.09.020

Reference yield:

: 65164-80-9
diphenyl 1-(phenylmethoxycarbonylamino)ethyl phosphonate

: 1346551-15-2
methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-dioxane; methanol

2: sodium iodide / acetone / 0.08 h / Reflux

With sodium iodide; In 1,4-dioxane; methanol; acetone;
DOI:10.1016/j.bmcl.2011.09.020

Reference yield:

: 621-84-1
O-benzyl carbamate

: 1346551-15-2
methyl hydrogen 1-(benzyloxycarbonylamino)ethyl phosphonate sodium salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / Cooling with ice

1.2: 1 h / 85 °C

2.1: 1,4-dioxane; methanol

3.1: sodium iodide / acetone / 0.08 h / Reflux

With acetic acid; sodium iodide; In 1,4-dioxane; methanol; acetone;
DOI:10.1016/j.bmcl.2011.09.020