C₂₆H₃₆O₄

Base Information

Chemical Name:C₂₆H₃₆O₄
CAS No.:1427005-39-7
Molecular Formula:C₂₆H₃₆O₄
Molecular Weight:412.569
Hs Code.:

C<sub>26</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:C₂₆H₃₆O₄

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Chemical Property of C₂₆H₃₆O₄

Chemical Property:

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Technology Process of C₂₆H₃₆O₄

There total 6 articles about C₂₆H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1427005-37-5
C₂₇H₃₈O₆

: 1427005-39-7
C₂₆H₃₆O₄

Guidance literature:: With hydrazine hydrate; potassium hydroxide; In diethylene glycol; at 130 - 220 ℃; for 11h; Dean-Stark; Inert atmosphere;
DOI:10.1021/ol4003724

Reference yield:

: (1R,2R,4S,6R,7R)-10-Bromo-4-((R)-1-hydroxy-2-methyl-propyl)-4,9,9-trimethoxy-3-oxa-tricyclo[5.2.2.0^2,6]undec-10-en-8-one

: 1427005-39-7
C₂₆H₃₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 0.17 h / 0 °C

1.2: 4.17 h / 0 - 80 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / 100 °C / Inert atmosphere

3.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / -78 °C

3.2: 5 h / -78 °C / Inert atmosphere

4.1: 18-crown-6 ether; potassium hexamethylsilazane / toluene / 20.5 h / 0 - 130 °C / Inert atmosphere

5.1: hydrazine hydrate; potassium hydroxide / diethylene glycol / 11 h / 130 - 220 °C / Dean-Stark; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cerium(III) chloride; 18-crown-6 ether; hydrazine hydrate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride; potassium hydroxide; In tetrahydrofuran; toluene; diethylene glycol; 3.1: |Grignard Reaction / 3.2: |Grignard Reaction / 4.1: |Oxy-Cope Rearrangement;
DOI:10.1021/ol4003724

Reference yield:

: 100-39-0
benzyl bromide

: 1427005-39-7
C₂₆H₃₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 0.17 h / 0 °C

1.2: 4.17 h / 0 - 80 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / 100 °C / Inert atmosphere

3.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / -78 °C

3.2: 5 h / -78 °C / Inert atmosphere

4.1: 18-crown-6 ether; potassium hexamethylsilazane / toluene / 20.5 h / 0 - 130 °C / Inert atmosphere

5.1: hydrazine hydrate; potassium hydroxide / diethylene glycol / 11 h / 130 - 220 °C / Dean-Stark; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cerium(III) chloride; 18-crown-6 ether; hydrazine hydrate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride; potassium hydroxide; In tetrahydrofuran; toluene; diethylene glycol; 3.1: |Grignard Reaction / 3.2: |Grignard Reaction / 4.1: |Oxy-Cope Rearrangement;
DOI:10.1021/ol4003724