Technology Process of C26H50O5Si2
There total 5 articles about C26H50O5Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
dichloromethane;
at -78 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ol302072b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene / 5 h / 80 °C / Inert atmosphere
2: AD-mix-α; methanesulfonamide / 1,4-dioxane; water / 48 h / 0 °C / Inert atmosphere
3: pyridine; silver nitrate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
4: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere
With
pyridine; methanesulfonamide; AD-mix-α; diisobutylaluminium hydride; silver nitrate;
In
1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/ol302072b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; silver nitrate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
2: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere
With
pyridine; diisobutylaluminium hydride; silver nitrate;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol302072b