4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)

Base Information

Chemical Name:4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)
CAS No.:1154426-01-3
Molecular Formula:C₂₄H₂₆N₄
Molecular Weight:370.497
Hs Code.:

Synonyms:4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)

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Chemical Property of 4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)

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Technology Process of 4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)

There total 2 articles about 4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1558-17-4
4,6-dimethylpyrimidine

: 100-10-7
4-dimethylamino-benzaldehyde

: 1154426-01-3
4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)

Guidance literature:: 4,6-dimethylpyrimidine; With potassium tert-butylate; In N,N-dimethyl-formamide; at 80 ℃; for 0.25h;

4-dimethylamino-benzaldehyde; In N,N-dimethyl-formamide; at 80 ℃; for 4h;
DOI:10.1021/jm300653b

Reference yield:

: 1558-17-4
4,6-dimethylpyrimidine

: 100-10-7
4-dimethylamino-benzaldehyde

: 1154425-79-2
(E)-4-(4-dimethylaminostyryl)-6-methylpyrimidine

: 1154426-01-3
4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 2h; Reflux; Inert atmosphere;
DOI:10.1021/jo900107u

Reference yield: 69.0%

: 1154426-01-3
4,4′-(1E,1′E)-2,2′-(pyrimidine-4,6-diyl)bis(ethene-2,1-diyl)bis(N,N-dimethylaniline)

: 586-77-6
4-bromo-N,N-dimethylaniline

: 4,4′,4″,4?-(pyrimidine-4,6-diylbis(ethene-2,1,1-triyl))tetrakis(N,N-dimethylaniline)

Guidance literature:: With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium acetate; potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 150 ℃; for 6h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.7b03024