(-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one

Base Information

Chemical Name:(-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one
CAS No.:84986-96-9
Molecular Formula:C₃₁H₂₉N₅O₄
Molecular Weight:535.602
Hs Code.:

Synonyms:(-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one

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Chemical Property of (-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one

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Technology Process of (-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one

There total 4 articles about (-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 14210-25-4
5-Chloro-1-phenyltetrazole

: 84960-89-4
(-)-1-(benzyloxy)-N-formyl-4-hydroxymorphinan-6-one

: 84986-96-9
(-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 18h; Ambient temperature;
DOI:10.1021/jo00157a016

Reference yield:

: 100-39-0
benzyl bromide

: 84986-96-9
(-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / K₂CO₃ / CHCl₃; methanol / 4 h / Heating

2: 64 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

With potassium carbonate; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jo00157a016

Reference yield:

: 76193-30-1
(-)-4-hydroxy-N-formylmorphinan-6-one

: 84986-96-9
(-)-1-(benzyloxy)-N-formyl-4-<(1-phenyl)-1H-tetrazol-5-yl)oxy>morphinan-6-one

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / NaH₂PO₄, Fremy's salt / methanol; H₂O / 1 h / Ambient temperature

2: 82 percent / zinc, NH₄Cl / methanol / 0.08 h / Heating

3: 48 percent / K₂CO₃ / CHCl₃; methanol / 4 h / Heating

4: 64 percent / K₂CO₃ / dimethylformamide / 18 h / Ambient temperature

With sodium dihydrogenphosphate; potassiuim nitrosodisulfonate; potassium carbonate; ammonium chloride; zinc; In methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00157a016