dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide

Base Information

Chemical Name:dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide
CAS No.:768369-96-6
Molecular Formula:C₃₉H₅₉N₃O
Molecular Weight:585.917
Hs Code.:

Synonyms:dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide

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Technology Process of dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide

There total 6 articles about dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 768370-00-9
1-{3-[4-(dibenzylaminobutyl)amino]propyl}-2-allylpiperidine

: 116902-88-6
9-decenoic acid chloride

: 768369-96-6
dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/jo049526i

Reference yield:

: 768369-98-8
N-acryloyl-2-allylpiperidine

: 768369-96-6
dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / toluene / 32 h / Heating

2: 90 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 228 mg / triethylamine / CH₂Cl₂ / 1 h / 0 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo049526i

Reference yield:

: 23608-88-0
2-(4-dibenzylaminobutyl)-isoindole-1,3-dione

: 768369-96-6
dec-9-enoic acid [3-(2-allyl-piperidin-1-yl)-propyl]-(4-dibenzylamino-butyl)-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / hydrazine monohydrate / ethanol / 3.5 h / Heating

2: 79 percent / toluene / 32 h / Heating

3: 90 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

4: 228 mg / triethylamine / CH₂Cl₂ / 1 h / 0 °C

With lithium aluminium tetrahydride; hydrazine hydrate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/jo049526i