3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

Base Information

Chemical Name:3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose
CAS No.:133508-14-2
Molecular Formula:C₂₆H₃₆O₅Si
Molecular Weight:456.654
Hs Code.:

Synonyms:3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

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Chemical Property of 3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

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Technology Process of 3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

There total 3 articles about 3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 134387-12-5
3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-5-O-(triphenylmethyl)-α-D-ribofuranose

: 133508-14-2
3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

Guidance literature:: With trichloroacetic acid; In dichloromethane; Ambient temperature;
DOI:10.1016/0008-6215(91)80095-5

Reference yield:

: 20590-54-9
1,2-O-isopropylidene-5-O-(triphenylmethyl)-α-D-erythro-pentofuranos-3-ulose

: 133508-14-2
3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH, 3) LiAlH₄

2: 98 percent / imidazole / dimethylformamide / Ambient temperature

3: 92 percent / trichloroacetic acid / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; sodium hydride; trichloroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)80095-5

Reference yield:

: 58399-76-1
3-Deoxy-3-C-(2'-hydroxyethyl)-1,2-O-isopropylidene-5-O-(triphenylmethyl)-α-D-ribofuranose

: 133508-14-2
3-C-<2'-O-(tert-butyldiphenylsilyloxy)ethyl>-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / imidazole / dimethylformamide / Ambient temperature

2: 92 percent / trichloroacetic acid / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; trichloroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)80095-5