(R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol

Base Information

Chemical Name:(R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol
CAS No.:215807-86-6
Molecular Formula:C₂₆H₃₂O₃SSi
Molecular Weight:452.69
Hs Code.:

Synonyms:(R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol

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Technology Process of (R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol

There total 2 articles about (R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 215807-84-4
1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-one

: 215807-86-6
(R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 1h;
DOI:10.1080/00397919808004924

Reference yield:

: 154698-92-7
methyl 2-((tert-butyl(diphenyl)silyl)oxy)acetate

: 215807-86-6
(R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / LDA / tetrahydrofuran / 1 h / -78 °C

2: 99 percent / DIBAL-H / toluene; tetrahydrofuran / 1 h / -78 °C

With diisobutylaluminium hydride; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.1080/00397919808004924

Reference yield:

: 215807-86-6
(R)-1-(tert-Butyl-diphenyl-silanyloxy)-3-((S)-toluene-4-sulfinyl)-propan-2-ol

: 106731-74-2,119944-29-5,107033-46-5
tert-butyl[(2S)-oxiran-2-ylmethoxy]diphenylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / 5 h / Heating

2: 87 percent / LiBH₄ / tetrahydrofuran / Ambient temperature

With lithium borohydride; sodium acetate; In tetrahydrofuran;
DOI:10.1080/00397919808004924