2-Hydrazinylisonicotinohydrazide

Base Information

• Chemical Name: 2-Hydrazinylisonicotinohydrazide
• CAS No.: 89465-51-0
• Molecular Formula: C₆H₉N₅O
• Molecular Weight: 167.17
• Mol file: 89465-51-0.mol

Synonyms:2-hydrazinylpyridine-4-carbohydrazide

Chemical Property of 2-Hydrazinylisonicotinohydrazide

Chemical Property:

• PKA: 11.47±0.20(Predicted)
• Density: 1.58±0.1 g/cm3(Predicted)
• Storage Temp.: Room temperature.

Purity/Quality:

≥95% ^*data from raw suppliers

2-Hydrazinylisonicotinohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Hydrazinylisonicotinohydrazide

There total 2 articles about 2-Hydrazinylisonicotinohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethyl 2-chloroisonicotinate (54453-93-9) → 2-hydrazinylpyridine-4-carbohydrazide (89465-51-0)

Guidance literature:

With hydrazine hydrate; In ethanol; water; at 160 ℃; for 1.5h; under 7500.75 - 11251.1 Torr; Microwave irradiation;

DOI:10.3390/molecules26185692

Reference yield:

→ 2-hydrazinylpyridine-4-carbohydrazide (89465-51-0)

Guidance literature:

2-Chlor-isonicotinsaeure, Hydrazinhydrat, sd. W.;

Reference yield:

2-hydrazinylpyridine-4-carbohydrazide (89465-51-0) + 2-nitroacetophenone (614-21-1) → (2-phenyl-5-(3-phenyl-[1,2,4]triazolo[4,3-a]pyridin-7-yl)-1,3,4-oxadiazole)

Guidance literature:

With 85% polyphosphoric acid; at 130 ℃;

DOI:10.3390/molecules26185692

upstream raw materials:

ethyl 2-chloroisonicotinate

Refernces