5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole

Base Information

Chemical Name:5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole
CAS No.:1449194-81-3
Molecular Formula:C₁₆H₁₅N₇O₂S
Molecular Weight:369.407
Hs Code.:

Synonyms:5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole

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Chemical Property of 5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole

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Technology Process of 5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole

There total 4 articles about 5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1449194-55-1
5-[(azidomethyl)thio]-1-phenyl-1H-tetrazole

: 866252-52-0
4,5-dimethoxy-2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1449194-81-3
5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole

Guidance literature:: With potassium fluoride; 18-crown-6 ether; In acetonitrile; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol401661j

Reference yield:

: 5-[(chloromethyl)thio]-1-phenyl-1H-tetrazole

: 1449194-81-3
5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium iodide / acetone / 4 h / Reflux

2: sodium azide / N,N-dimethyl-formamide / 4 h / 50 °C

3: 18-crown-6 ether; potassium fluoride / acetonitrile / 4 h / 20 °C

With potassium fluoride; sodium azide; 18-crown-6 ether; sodium iodide; In N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ol401661j

Reference yield:

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1449194-81-3
5,6-dimethoxy-1-{[(1-phenyl-1H-tetrazol-5-yl)thio]methyl}-1H-benzo[d][1,2,3]triazole

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 3 h / Reflux

2: sodium iodide / acetone / 4 h / Reflux

3: sodium azide / N,N-dimethyl-formamide / 4 h / 50 °C

4: 18-crown-6 ether; potassium fluoride / acetonitrile / 4 h / 20 °C

With potassium fluoride; sodium azide; 18-crown-6 ether; potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ol401661j