Technology Process of C51H57NO13
There total 4 articles about C51H57NO13 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C31H36O9; (3R,4S)-3-(1-ethoxyethoxy)-4-(phenyl)-N-benzoyl-2-azetidinone;
With
sodium hexamethyldisilazane;
In
tetrahydrofuran;
at -78 ℃;
for 0.5h;
Inert atmosphere;
With
water; ammonium chloride;
In
tetrahydrofuran;
Inert atmosphere;
DOI:10.1021/jm400479p
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 10 h / -40 °C / Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 8 h / 20 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
4.2: Inert atmosphere
With
1H-imidazole; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm400479p
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: Inert atmosphere
With
tetrabutyl ammonium fluoride; sodium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1021/jm400479p