9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate

Base Information

Chemical Name:9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate
CAS No.:1254972-58-1
Molecular Formula:BF₄*C₃₄H₂₁N₂
Molecular Weight:544.359
Hs Code.:

Synonyms:9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate

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Chemical Property of 9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate

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Technology Process of 9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate

There total 1 articles about 9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1254972-54-7
9-(4'-bromophenyl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate

: 98-80-6
phenylboronic acid

: 1254972-58-1
9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In N,N-dimethyl-formamide; at 150 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ja108668h

Reference yield: 85.0%

: 1254972-58-1
9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate

: 333-27-7
methyl trifluoromethanesulfonate

: 9-(biphenyl-4-yl)-2-methyl-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-2,15-diium bis-hexafluorophosphate

Guidance literature:: 9-(biphenyl-4-yl)-benzo[c]benzo[1,2]quinolizino[3,4,5,6-ija][1,6]naphthyridin-15-ium tetrafluoroborate; methyl trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

With potassium hexafluorophosphate; In water; acetonitrile; Inert atmosphere;
DOI:10.1021/ja108668h