(3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene

Base Information

• Chemical Name: (3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene
• CAS No.: 108120-42-9
• Molecular Formula: C₂₀H₁₈N₂O
• Molecular Weight: 302.376

Synonyms:(3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene

Chemical Property of (3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene

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Technology Process of (3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene

There total 1 articles about (3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2-((E)-3-phenyl-allyloxy)-naphthalene-1-carbaldehyde (108120-32-7) → (3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene (108120-42-9)

Guidance literature:

With hydrazine dihydrochloride; In ethanol; for 4h; Heating;

DOI:10.1021/jo00387a031

Reference yield: 95.0%

(3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene (108120-42-9) + acetyl chloride (75-36-5) → 1,2-diacetyl-1,2,3,3a,4,11c-hexahydronaphtho<1',2',:5,6>pyrano<4,3-c>pyrazole (108120-47-4)

Guidance literature:

With triethylamine; In chloroform; for 2h; Heating;

DOI:10.1021/jo00387a031

Reference yield:

2-((E)-3-phenyl-allyloxy)-naphthalene-1-carbaldehyde (108120-32-7) + (3R,3aS,11cR)-3-Phenyl-1,2,3,3a,4,11c-hexahydro-5-oxa-1,2-diaza-cyclopenta[c]phenanthrene (108120-42-9) → C40H32N2O2*ClH

Guidance literature:

With hydrogenchloride; In ethanol; for 3h; Heating;

DOI:10.1021/jo00387a031

upstream raw materials:

2-((E)-3-phenyl-allyloxy)-naphthalene-1-carbaldehyde

Downstream raw materials:

1,2-diacetyl-1,2,3,3a,4,11c-hexahydronaphtho<1',2',:5,6>pyrano<4,3-c>pyrazole

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