(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate

Base Information

Chemical Name:(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate
CAS No.:1227514-63-7
Molecular Formula:C₂₂H₃₇NO₅Si
Molecular Weight:423.625
Hs Code.:

Synonyms:(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate

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Chemical Property of (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate

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Technology Process of (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate

There total 1 articles about (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1227514-62-6
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-ol

: 3019-71-4
Trichloroacetyl isocyanate

: 1227514-63-7
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate

Guidance literature:: (3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-ol; Trichloroacetyl isocyanate; In dichloromethane; at 0 ℃; Inert atmosphere;

With water; potassium carbonate; In methanol; at 0 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2010.02.093

Reference yield: 15.0%

: 1227514-63-7
(3S,5R)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-hept-1-en-3-yl carbamate

: 1227514-64-8
5-((R)-2-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)butyl)-4-(hydroxymethyl)oxazolidin-2-one

Guidance literature:: With potassium osmate(VI); tert-butylhypochlorite; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In propan-1-ol; for 2.5h;
DOI:10.1016/j.tet.2010.02.093