{4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Base Information

Chemical Name:{4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester
CAS No.:350717-03-2
Molecular Formula:C₂₉H₃₂F₁₇N₃O₃
Molecular Weight:793.564
Hs Code.:

Synonyms:{4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

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Chemical Property of {4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

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Technology Process of {4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

There total 5 articles about {4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 26116-12-1
1-ethyl-2-pyrrolidinemethanamine

: 350716-69-7
4-[(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethylundecyloxycarbonylamino)-methyl]benzoic acid

: 350717-03-2
{4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In chloroform; N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/jo010111w

Reference yield:

: 2-[2-(1H,1H,2H,2H-perfluorodecyl)isopropoxycarbonyloxyimino]-2-phenylacetonitrile

: 350717-03-2
{4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / Et₃N / tetrahydrofuran; H₂O / 20 °C

2: 94 percent / EDCI; HOBt; Et₃N / CHCl₃; dimethylformamide / 16 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jo010111w

Reference yield:

: 56-91-7
p-aminomethylbenzoic acid

: 350717-03-2
{4-[(1-ethyl-pyrrolidin-2-ylmethyl)-carbamoyl]-benzyl}-carbamic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-1,1-dimethyl-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / Et₃N / tetrahydrofuran; H₂O / 20 °C

2: 94 percent / EDCI; HOBt; Et₃N / CHCl₃; dimethylformamide / 16 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jo010111w