Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ⁵-phosphanylidene)-propyl]-phosphonium; bromide

Base Information

• Chemical Name: Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ⁵-phosphanylidene)-propyl]-phosphonium; bromide
• CAS No.: 39898-85-6
• Molecular Formula: Br*C₄₅H₃₈NP₂
• Molecular Weight: 734.655

Synonyms:Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ⁵-phosphanylidene)-propyl]-phosphonium; bromide

Chemical Property of Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ⁵-phosphanylidene)-propyl]-phosphonium; bromide

Chemical Property:

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Technology Process of Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ⁵-phosphanylidene)-propyl]-phosphonium; bromide

There total 1 articles about Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ⁵-phosphanylidene)-propyl]-phosphonium; bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triphenyl(prop-2-ynyl)phosphonium bromide (2091-46-5) + N-phenyltriphenyliminophosphorane (2325-27-1) → Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ5-phosphanylidene)-propyl]-phosphonium; bromide (39898-85-6)

Guidance literature:

for 40h; Ambient temperature;

DOI:10.1016/S0040-4039(01)80602-X

Reference yield: 95.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ5-phosphanylidene)-propyl]-phosphonium; bromide (39898-85-6) → 2-Anilinobuta-1,3-dienyl(triphenyl)phosphonium Bromide (126404-73-7)

Guidance literature:

In dichloromethane; at 25 ℃; for 1h;

DOI:10.1016/S0040-4039(01)80602-X

Reference yield: 93.0%

benzaldehyde (100-52-7) + Triphenyl-[2-[(Z)-phenylimino]-3-(triphenyl-λ5-phosphanylidene)-propyl]-phosphonium; bromide (39898-85-6) → Triphenyl-((1E,3E)-4-phenyl-2-phenylamino-buta-1,3-dienyl)-phosphonium; bromide (126404-68-0)

Guidance literature:

In dichloromethane; at 25 ℃; for 14h;

DOI:10.1016/S0040-4039(01)80602-X

upstream raw materials:

triphenyl(prop-2-ynyl)phosphonium bromide

N-phenyltriphenyliminophosphorane

Downstream raw materials:

2-Anilino-4-(2-furyl)buta-1,3-dienyl(triphenyl)phosphonium Bromide

2-Anilinobuta-1,3-dienyl(triphenyl)phosphonium Bromide

2-Anilino-4-(p-tolyl)buta-1,3-dienyl(triphenyl)phosphonium Bromide

Triphenyl-((1E,3E)-4-phenyl-2-phenylamino-buta-1,3-dienyl)-phosphonium; bromide

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