(2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

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Chemical Name:(2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol
CAS No.:850249-39-7
Molecular Formula:C₄₀H₄₀N₂O₁₀S₂
Molecular Weight:772.897
Hs Code.:

(2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

Synonyms:(2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

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Chemical Property of (2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

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Technology Process of (2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

There total 3 articles about (2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 850249-37-5
6-[2-(1-benzenesulfonyl-1H-indol-3-yl)-ethoxy]-2-(1-benzenesulfonyl-1H-pyrrol-2-yl)-8-benzyloxy-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 850249-39-7
(2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; at 20 ℃;
DOI:10.1021/ol050119i

Reference yield:

: 850249-34-2
N-phenylsulfonylpyrrole-2-carboxaldehyde diethylacetal

: 850249-39-7
(2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / pyridinium p-toluenesulfonic acid / CHCl₃ / 80 °C

2: 55 percent / HCl; sodium cyanoborohydride / dioxane; tetrahydrofuran / 20 °C

With hydrogenchloride; pyridinium p-toluenesulfonate; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; chloroform;
DOI:10.1021/ol050119i

Reference yield:

: 86688-93-9
1-benzenesulfonyl-2-formylpyrrole

: 850249-39-7
(2R,3R,4S,5R,6R)-2-[2-(1-Benzenesulfonyl-1H-indol-3-yl)-ethoxy]-6-(1-benzenesulfonyl-1H-pyrrol-2-ylmethoxymethyl)-4-benzyloxy-tetrahydro-pyran-3,5-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Amberlyst-25 resin / 24 h

2: 99 percent / pyridinium p-toluenesulfonic acid / CHCl₃ / 80 °C

3: 55 percent / HCl; sodium cyanoborohydride / dioxane; tetrahydrofuran / 20 °C

With hydrogenchloride; Amberlyst-25 resin; pyridinium p-toluenesulfonate; sodium cyanoborohydride; In tetrahydrofuran; 1,4-dioxane; chloroform;
DOI:10.1021/ol050119i