Technology Process of C30H25N5O6
There total 10 articles about C30H25N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H19BrN4O3; C17H20BNO5;
With
caesium carbonate;
In
1,4-dioxane; ethanol; water;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; ethanol; water;
at 90 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium hydroxide; water / ethanol / 2 h / Reflux
1.2: 16 h
2.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
2.2: 16 h / 0 - 20 °C
3.1: caesium carbonate / ethanol; water; 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere
3.2: 12 h / 90 °C
With
water; benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; potassium hydroxide;
In
1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.33 h / 20 °C / Inert atmosphere
1.2: 16 h / 0 - 20 °C
2.1: caesium carbonate / ethanol; water; 1,4-dioxane / 0.5 h / 20 °C / Inert atmosphere
2.2: 12 h / 90 °C
With
benzotriazol-1-ol; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;