(1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

Base Information

Chemical Name:(1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane
CAS No.:97747-52-9
Molecular Formula:C₁₅H₂₁BrO₈
Molecular Weight:409.231
Hs Code.:

Synonyms:(1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

Suppliers and Price of (1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

There total 4 articles about (1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90760-56-8
(-)-7-endo-oxabicyclo<2.2.1>hept-5-ene-2-carboxylic acid

: 97747-52-9
(1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / 90percent formic acid, 35percent hydrogen peroxide / 0.33 h / 70 °C

2: 1) lithium aluminium hydride / 1) THF, RT, 30 min, 2) pyridine, RT, 1 h

3: 53 percent / 20percent hydrogen bromide / acetic acid / 20 h / 85 °C

With lithium aluminium tetrahydride; formic acid; hydrogen bromide; dihydrogen peroxide; In acetic acid;
DOI:10.1039/P19850000903

Reference yield:

: 97747-50-7
(3R)-(+)-2-exo-hydroxy-4,8-dioxatricyclo<4.2.1.0^3,7>nonan-5-one

: 97747-52-9
(1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 1) lithium aluminium hydride / 1) THF, RT, 30 min, 2) pyridine, RT, 1 h

2: 53 percent / 20percent hydrogen bromide / acetic acid / 20 h / 85 °C

With lithium aluminium tetrahydride; hydrogen bromide; In acetic acid;
DOI:10.1039/P19850000903

Reference yield:

: 90695-20-8
(1S)-2-exo,3-endo-diacetoxy-5-endo-acetoxymethyl-7-oxabicyclo<2.2.1.>heptane

: 97747-52-9
(1R)-(-)-(1,3,5/2,4)-2,3,4-triacetoxy-1-acetoxymethyl-5-bromocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / 20percent hydrogen bromide / acetic acid / 20 h / 85 °C

With hydrogen bromide; In acetic acid;
DOI:10.1039/P19850000903