2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

Base Information

Chemical Name:2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one
CAS No.:83849-51-8
Molecular Formula:C₁₉H₂₈O₃
Molecular Weight:304.43
Hs Code.:

Synonyms:2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

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Chemical Property of 2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

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Technology Process of 2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

There total 1 articles about 2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83849-46-1,83997-80-2,99032-30-1,99032-31-2
2,2-Dimethyl-1-(2-methylprop-1-enyl)-cis-3-(2-p-tolyl-2-hydroxypropyl)-cyclopropane

: 83849-49-4,83915-91-7,98975-71-4,98975-72-5
(1R,3S)-3-(2-Hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropanecarboxylic acid

: 83849-51-8
2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

Guidance literature:: With potassium permanganate; acetic acid; In water; acetone; at 30 ℃; for 2h;

Reference yield: 79.5%

: 83849-51-8
2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

: 83849-52-9
2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

Guidance literature:: With sodium tetrahydroborate; In methanol; for 65h;

Reference yield:

: 83849-51-8
2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

: (1R,3S)-2,2-Dimethyl-3-(2-p-tolyl-allyl)-cyclopropanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 79.5 percent / NaBH₄ / methanol / 65 h

2: 1 g / Jones' chromic acid reagent / acetone / 2 h / 0 °C

3: diethyl ether

4: POCl₃, pyridine / 1) 0-5 deg C 2) 10 deg C, 24h

With pyridine; sodium tetrahydroborate; chromic acid; trichlorophosphate; In methanol; diethyl ether; acetone;