2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

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Chemical Name:2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane
CAS No.:83849-52-9
Molecular Formula:C₁₉H₃₀O₃
Molecular Weight:306.445
Hs Code.:

Synonyms:2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

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Chemical Property of 2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

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Technology Process of 2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

There total 1 articles about 2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.5%

: 83849-51-8
2-Hydroxy-1-[(1R,3S)-3-(2-hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropyl]-2-methyl-propan-1-one

: 83849-52-9
2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

Guidance literature:: With sodium tetrahydroborate; In methanol; for 65h;

Reference yield:

: 83849-52-9
2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

: 83849-49-4,83915-91-7,98975-71-4,98975-72-5
(1R,3S)-3-(2-Hydroxy-2-p-tolyl-propyl)-2,2-dimethyl-cyclopropanecarboxylic acid

Guidance literature:: With chromic acid; In acetone; at 0 ℃; for 2h; Further byproducts given;

Reference yield:

: 83849-52-9
2,2-Dimethyl-3-(2-p-tolyl-2-hydroxypropyl)-cis-1-(2-methyl-1,2-dihydroxypropyl)cyclopropane

: (1R,3S)-2,2-Dimethyl-3-(2-p-tolyl-allyl)-cyclopropanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1 g / Jones' chromic acid reagent / acetone / 2 h / 0 °C

2: diethyl ether

3: POCl₃, pyridine / 1) 0-5 deg C 2) 10 deg C, 24h

With pyridine; chromic acid; trichlorophosphate; In diethyl ether; acetone;