Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

Base Information

Chemical Name:Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester
CAS No.:252042-33-4
Molecular Formula:C₃₆H₅₆Cl₃NO₁₀
Molecular Weight:769.2
Hs Code.:

Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

Synonyms:Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

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Chemical Property of Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

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Technology Process of Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

There total 4 articles about Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Hexanoic acid (R)-1-{[(4aR,6R,7R,8R,8aS)-6-benzyloxy-2,2-dimethyl-8-(2,2,2-trichloro-ethoxycarbonyloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl]-methyl}-dodecyl ester

: 252042-33-4
Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

Guidance literature:: With acetic acid; at 60 ℃; for 1h;
DOI:10.1021/jm990222b

Reference yield:

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 252042-33-4
Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide methiodide / CH₂Cl₂ / 20 °C

2: 4-(dimethylamino)pyridine; pyridine / CH₂Cl₂ / 3 h / 20 °C

3: 80 percent aq. AcOH / 1 h / 60 °C

With pyridine; dmap; 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; acetic acid; In dichloromethane; 1: Acylation / 2: Acylation / 3: Hydrolysis;
DOI:10.1021/jm990222b

Reference yield:

: (R)-3-hexanoyloxytetradecanoic acid

: 252042-33-4
Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide methiodide / CH₂Cl₂ / 20 °C

2: 4-(dimethylamino)pyridine; pyridine / CH₂Cl₂ / 3 h / 20 °C

3: 80 percent aq. AcOH / 1 h / 60 °C

With pyridine; dmap; 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; acetic acid; In dichloromethane; 1: Acylation / 2: Acylation / 3: Hydrolysis;
DOI:10.1021/jm990222b