Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester

Base Information

Chemical Name:Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester
CAS No.:252042-28-7
Molecular Formula:C₃₆H₅₉NO₈
Molecular Weight:633.866
Hs Code.:

Synonyms:Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester

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Chemical Property of Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester

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Technology Process of Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester

There total 1 articles about Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: (R)-3-hexanoyloxytetradecanoic acid

: 252042-28-7
Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester

Guidance literature:: With 3-{[(ethylimino)methylene]-amino}-N,N,N-trimethyl-1-propanaminium iodide; In dichloromethane; at 20 ℃;
DOI:10.1021/jm990222b

Reference yield:

: 252042-28-7
Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: Hexanoic acid (R)-1-{[(4aR,6R,7R,8R,8aS)-6-benzyloxy-2,2-dimethyl-8-(2,2,2-trichloro-ethoxycarbonyloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl]-methyl}-dodecyl ester

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jm990222b

Reference yield:

: 252042-28-7
Hexanoic acid (R)-1-[((4aR,6R,7R,8R,8aS)-6-benzyloxy-8-hydroxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ylcarbamoyl)-methyl]-dodecyl ester

: 252042-33-4
Hexanoic acid (R)-1-{[(2R,3R,4R,5S,6R)-2-benzyloxy-5-hydroxy-6-hydroxymethyl-4-(2,2,2-trichloro-ethoxycarbonyloxy)-tetrahydro-pyran-3-ylcarbamoyl]-methyl}-dodecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine; pyridine / CH₂Cl₂ / 3 h / 20 °C

2: 80 percent aq. AcOH / 1 h / 60 °C

With pyridine; dmap; acetic acid; In dichloromethane; 1: Acylation / 2: Hydrolysis;
DOI:10.1021/jm990222b