all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.0^4,10>decan-2,5,8-triamine

Base Information

• Chemical Name: all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.0^4,10>decan-2,5,8-triamine
• CAS No.: 136869-72-2
• Molecular Formula: C₄₉H₇₃N₃O₁₂
• Molecular Weight: 896.132

Synonyms:all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.0^4,10>decan-2,5,8-triamine

Chemical Property of all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.0^4,10>decan-2,5,8-triamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.0^4,10>decan-2,5,8-triamine

There total 6 articles about all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.0^4,10>decan-2,5,8-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

8-(o-methoxyphenoxy)-3,6-dioxaoctylamine (136869-75-5) + all-cis-tricyclo<5.2.1.04,10>decane-2,5,8-trione (78168-48-6,118627-08-0,118627-20-6,136891-83-3) → all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.04,10>decan-2,5,8-triamine (136869-72-2)

Guidance literature:

With hydrogen; 10% palladium on active carbon; In methanol; for 72h; under 760 Torr; Ambient temperature;

DOI:10.1016/S0040-4020(01)86537-6

Reference yield:

2-[2-(chloroethoxy)ethoxy]ethanol (5197-62-6) → all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.04,10>decan-2,5,8-triamine (136869-72-2)

Guidance literature:

Multi-step reaction with 5 steps

1: KOH / butan-1-ol / 20 h / Heating

2: 65 percent / pyridine / 20 °C

3: 76 percent / sodium azide / tetrabutylammonium bromide / H₂O / 20 h / Heating

4: 77 percent / H₂ / 10percentPd-C / methanol / 12 h / 760 Torr / Ambient temperature

5: 55 percent / H₂ / 10percentPd-C / methanol / 72 h / 760 Torr / Ambient temperature

With pyridine; potassium hydroxide; sodium azide; hydrogen; 10% palladium on active carbon; tetrabutylammomium bromide; In methanol; water; butan-1-ol;

DOI:10.1016/S0040-4020(01)86537-6

Reference yield:

1-azido-8-(o-methoxyphenoxy)3,6-dioxaoctane (136869-74-4) → all-cis,tris-endo-N,N',N-tris-(8-o-methoxyphenoxy-3,6-dioxaoctyl)tricyclo<5.2.1.04,10>decan-2,5,8-triamine (136869-72-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / H₂ / 10percentPd-C / methanol / 12 h / 760 Torr / Ambient temperature

2: 55 percent / H₂ / 10percentPd-C / methanol / 72 h / 760 Torr / Ambient temperature

With hydrogen; 10% palladium on active carbon; In methanol;

DOI:10.1016/S0040-4020(01)86537-6

upstream raw materials:

8-(o-methoxyphenoxy)-3,6-dioxaoctylamine

all-cis-tricyclo<5.2.1.0^4,10>decane-2,5,8-trione

2-[2-(chloroethoxy)ethoxy]ethanol

1-azido-8-(o-methoxyphenoxy)3,6-dioxaoctane

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