vinyl isopropyl-4-methoxyphenylcarbamate

Base Information

Chemical Name:vinyl isopropyl-4-methoxyphenylcarbamate
CAS No.:1350911-17-9
Molecular Formula:C₁₃H₁₇NO₃
Molecular Weight:235.283
Hs Code.:

Synonyms:vinyl isopropyl-4-methoxyphenylcarbamate

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Chemical Property of vinyl isopropyl-4-methoxyphenylcarbamate

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Technology Process of vinyl isopropyl-4-methoxyphenylcarbamate

There total 3 articles about vinyl isopropyl-4-methoxyphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1350911-11-3
N-isopropyl-N-(4-mthoxyphenyl)carbamoylchloride

: 675825-21-5
Lithium enolate of the acetaldehyde

: 1350911-17-9
vinyl isopropyl-4-methoxyphenylcarbamate

Guidance literature:: In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol2029355

Reference yield:

: 16495-67-3
4-(isopropylamino)anisole

: 1350911-17-9
vinyl isopropyl-4-methoxyphenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 4 h / 20 °C / Inert atmosphere

With pyridine; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; dichloromethane;
DOI:10.1021/ol2029355

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1350911-17-9
vinyl isopropyl-4-methoxyphenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / acetic acid; 1,2-dichloro-ethane / 4 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / 4 h / 20 °C / Inert atmosphere

With pyridine; sodium tris(acetoxy)borohydride; In 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; dichloromethane; acetic acid; 1,2-dichloro-ethane;
DOI:10.1021/ol2029355