C₄₈H₅₂N₄O₈Si

Base Information

Chemical Name:C₄₈H₅₂N₄O₈Si
CAS No.:1386972-47-9
Molecular Formula:C₄₈H₅₂N₄O₈Si
Molecular Weight:841.048
Hs Code.:

C<sub>48</sub>H<sub>52</sub>N<sub>4</sub>O<sub>8</sub>Si

Synonyms:C₄₈H₅₂N₄O₈Si

Suppliers and Price of C₄₈H₅₂N₄O₈Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₈H₅₂N₄O₈Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₈H₅₂N₄O₈Si

There total 10 articles about C₄₈H₅₂N₄O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1383446-30-7
thiotolyl 3-O-acetyl-2-azido-4-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside

: 105496-31-9
N-(9-fluorenylmethoxycarbonyl)-2-aminoethanol

: 1386972-45-7
2'-(9H-fluoren-9-yl)methoxycarbonylaminoethyl-3-O-acetyl-2-azido-4-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-α-D-glucopyranoside

: 1386972-47-9
C₄₈H₅₂N₄O₈Si

Guidance literature:: thiotolyl 3-O-acetyl-2-azido-4-O-benzyl-6-O-(tert-butyldiphenylsilyl)-2-deoxy-β-D-glucopyranoside; N-(9-fluorenylmethoxycarbonyl)-2-aminoethanol; In toluene; for 1h;

In diethyl ether; 1,2-dichloro-ethane; at -20 - 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trifluorormethanesulfonic acid; at -20 ℃; for 5h; optical yield given as %de;
DOI:10.1080/07328303.2012.658274

Reference yield:

: thiotolyl 3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 1386972-47-9
C₄₈H₅₂N₄O₈Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,6-dimethylpyridine; di-n-butylboryl trifluoromethanesulfonate; diborane / tetrahydrofuran / 10 h / 0 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C

3.1: toluene / 1 h

3.2: 1 h / -20 - 20 °C / Molecular sieve; Inert atmosphere

3.3: 5 h / -20 °C

With 1H-imidazole; 2,6-dimethylpyridine; di-n-butylboryl trifluoromethanesulfonate; diborane; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1080/07328303.2012.658274

Reference yield:

: 1386972-44-6
C₂₂H₂₅N₃O₅S

: 1386972-47-9
C₄₈H₅₂N₄O₈Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 20 °C

2.1: toluene / 1 h

2.2: 1 h / -20 - 20 °C / Molecular sieve; Inert atmosphere

2.3: 5 h / -20 °C

With 1H-imidazole; In N,N-dimethyl-formamide; toluene;
DOI:10.1080/07328303.2012.658274