deuterio ferrocenecarboxaldehyde

Base Information

Chemical Name:deuterio ferrocenecarboxaldehyde
CAS No.:59561-88-5
Molecular Formula:C₁₁H₁₀FeO
Molecular Weight:215.039
Hs Code.:

Synonyms:deuterio ferrocenecarboxaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of deuterio ferrocenecarboxaldehyde

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Technology Process of deuterio ferrocenecarboxaldehyde

There total 1 articles about deuterio ferrocenecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-54-5,55404-68-7
ferrocene

: 2914-27-4
d1-N,N-dimethylformamide

: 59561-88-5
deuterio ferrocenecarboxaldehyde

Guidance literature:: With t-butyl lithium; aq. HCl; In tetrahydrofuran; pentane; ferrocene placed in a flask at -20°C, passed N2, added dry THF, stirred for 15 min, added LiC(CH3)3 in pentane over 15 min, stirred for 40 min, warmed to -10°C, added a soln. (THF) of dimethylformamide,left for 40 min, added aq. HCl; the solvent removed at 55°C with a slow decrease in pressure from1 atm to 0.5 torr, added N2 (brought back to atm. pressure), inserted a cold-water finger, sublimed the solid at 0.5 torr and 75°C, the crystals removed from the cold finger;
DOI:10.1063/1.1993593