N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea

Base Information

• Chemical Name: N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea
• CAS No.: 1067181-10-5
• Molecular Formula: C₂₀H₂₃N₃O₅S₂
• Molecular Weight: 449.552

Synonyms:N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea

Chemical Property of N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea

Chemical Property:

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Technology Process of N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea

There total 1 articles about N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

N-[(2,4,6-trimethylphenyl)sulfonyl]-(S)-methylisothiourea (930121-59-8) + benzyloxycarbonyl isocyanate (69032-16-2) → N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea (1067181-10-5)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja804607v

Reference yield: 94.4%

N-[(2,4,6-trimethylphenyl)sulfonyl]-N'-benzyloxycarbonyl-(S)-methylisothiourea (1067181-10-5) + glycine tert-butyl ester hydrochloride (27532-96-3) → 2-[6-(2,4,6-trimethylphenyl)sulfonylamino-3,4-dihydro-2,4-dioxo-1,3,5-triazin-1(2H)-yl]acetic acid t-butyl ester (1067181-11-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 45 ℃; for 21.1667h;

DOI:10.1021/ja804607v

upstream raw materials:

N-[(2,4,6-trimethylphenyl)sulfonyl]-(S)-methylisothiourea

benzyloxycarbonyl isocyanate

Downstream raw materials:

2-[6-(2,4,6-trimethylphenyl)sulfonylamino-3,4-dihydro-2,4-dioxo-1,3,5-triazin-1(2H)-yl]acetic acid t-butyl ester

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