C₃₃H₃₈FN₅O₆S

Base Information

Chemical Name:C₃₃H₃₈FN₅O₆S
CAS No.:868286-93-5
Molecular Formula:C₃₃H₃₈FN₅O₆S
Molecular Weight:651.759
Hs Code.:

C<sub>33</sub>H<sub>38</sub>FN<sub>5</sub>O<sub>6</sub>S

Synonyms:C₃₃H₃₈FN₅O₆S

Suppliers and Price of C₃₃H₃₈FN₅O₆S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₃₈FN₅O₆S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₃₈FN₅O₆S

There total 15 articles about C₃₃H₃₈FN₅O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₀FN₅O₇S

: 868286-93-5
C₃₃H₃₈FN₅O₆S

Guidance literature:: With sodium acetate; In ethanol; water; at 86 ℃; for 16h;

Reference yield:

: 695216-00-3
3-[(methylsulfonyl)amino]-5-nitrobenzoic acid methyl ester

: 868286-93-5
C₃₃H₃₈FN₅O₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 3 h / 20 °C

2.1: methanol; sodium hydroxide / tetrahydrofuran / 1.5 h / 20 °C

2.2: 20 °C / pH < 1

3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 65 h / 20 °C

4.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

5.1: tetrafluoroboric acid / water; acetonitrile / 0.67 h / 0 - 20 °C

5.2: 1 h / 0 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / DMF (N,N-dimethyl-formamide) / 0.5 h / 180 °C / Microwave

7.1: hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol / 0.08 h / 130 °C / Microwave

8.1: benzotriazol-1-ol; diisopropyl-carbodiimide / DMF (N,N-dimethyl-formamide); dichloromethane / 1.5 h / 20 °C

9.1: sodium acetate / ethanol; water / 16 h / 86 °C

With methanol; sodium hydroxide; tetrafluoroboric acid; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; water; hydrogen; sodium acetate; sodium hydride; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; diisopropyl-carbodiimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 695216-01-4
3-[methyl(methylsulfonyl)amino]-5-nitrobenzoic acid methyl ester

: 868286-93-5
C₃₃H₃₈FN₅O₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: methanol; sodium hydroxide / tetrahydrofuran / 1.5 h / 20 °C

1.2: 20 °C / pH < 1

2.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 65 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 16 h

4.1: tetrafluoroboric acid / water; acetonitrile / 0.67 h / 0 - 20 °C

4.2: 1 h / 0 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / DMF (N,N-dimethyl-formamide) / 0.5 h / 180 °C / Microwave

6.1: hydroxylamine hydrochloride; water; potassium carbonate; isopropyl alcohol / 0.08 h / 130 °C / Microwave

7.1: benzotriazol-1-ol; diisopropyl-carbodiimide / DMF (N,N-dimethyl-formamide); dichloromethane / 1.5 h / 20 °C

8.1: sodium acetate / ethanol; water / 16 h / 86 °C

With methanol; sodium hydroxide; tetrafluoroboric acid; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; water; hydrogen; sodium acetate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isopropyl alcohol; diisopropyl-carbodiimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; acetonitrile;