(5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester

Base Information

• Chemical Name: (5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester
• CAS No.: 62439-94-5
• Molecular Formula: C₃₁H₃₄O₇
• Molecular Weight: 518.607

Synonyms:(5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester

Chemical Property of (5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester

Chemical Property:

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Technology Process of (5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester

There total 2 articles about (5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(5Z,13E)-(8R,9S,11R,12R)-9,11-Dihydroxy-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester (62473-17-0) + benzoyl chloride (98-88-4) → (5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester (62439-94-5)

Guidance literature:

With pyridine; sodium hydrogencarbonate; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; sulfuric acid;

Reference yield:

(Z)-7-{(1R,2R,3R,5S)-3,5-Dihydroxy-2-[(E)-2-(2,5,5-trimethyl-[1,3]dioxan-2-yl)-vinyl]-cyclopentyl}-hept-5-enoic acid methyl ester → (5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester (62439-94-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid

2: pyridine

With pyridine; acetic acid;

Reference yield:

(5Z, 13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester (62439-94-5) → (8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostanoic Acid Methyl Ester (62440-37-3)

Guidance literature:

With hydrogen; palladium on activated charcoal;

upstream raw materials:

(5Z,13E)-(8R,9S,11R,12R)-9,11-Dihydroxy-15-oxo-17,18,19,20-tetranor-prostadienoic Acid Methyl Ester

benzoyl chloride

Downstream raw materials:

(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostanoic Acid Methyl Ester

(13E)-(8R,9S,11R,12R)-9,11-Bis(benzoyloxy)-15-oxo-17,18,19,20-tetranor-prostenoic Acid Methyl Ester

C₃₉H₄₀O₇

C₃₆H₄₆O₇

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