2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Base Information

Chemical Name:2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene
CAS No.:881199-44-6
Molecular Formula:C₂₆H₃₄O₅
Molecular Weight:426.553
Hs Code.:

Synonyms:2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

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Technology Process of 2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

There total 6 articles about 2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 494798-06-0
2-allyl-3-ethoxy-4-methoxybenzyl alcohol

: 767290-03-9
2-allyl-3-isopropoxy-4-methoxyphenol

: 881199-44-6
2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.3987/COM-05-10592

Reference yield:

: 621-59-0
isovanillin

: 881199-44-6
2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / K₂CO₃ / acetone / 8 h / Heating

2: 92 percent / 3 h / 180 °C

3: K₂CO₃ / acetone / 8 h / Heating

4: sodium borohydride / ethanol / 0.5 h / 20 °C

5: 54 percent / triphenylphosphane; diisopropyl diazenedicarboxylate / tetrahydrofuran / 12 h / 20 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; ethanol; acetone; 2: Claisen rearrangement / 5: Mitsunobu reaction;
DOI:10.3987/COM-05-10592

Reference yield:

: 18075-40-6
O-allylisovanillin

: 881199-44-6
2-allyl-1-[(2-allyl-3-ethoxy-4-methoxybenzyl)oxy]-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / 3 h / 180 °C

2: K₂CO₃ / acetone / 8 h / Heating

3: sodium borohydride / ethanol / 0.5 h / 20 °C

4: 54 percent / triphenylphosphane; diisopropyl diazenedicarboxylate / tetrahydrofuran / 12 h / 20 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; ethanol; acetone; 1: Claisen rearrangement / 4: Mitsunobu reaction;
DOI:10.3987/COM-05-10592