1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

Base Information

Chemical Name:1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol
CAS No.:101069-26-5
Molecular Formula:C₂₅H₃₄O₅Si
Molecular Weight:442.627
Hs Code.:

Synonyms:1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

Chemical Property:

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Technology Process of 1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

There total 2 articles about 1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7726-97-8,10334-28-8,20662-31-1,22554-76-3,22554-77-4,22554-79-6,27299-12-3,28218-56-6,32742-35-1,40026-08-2,51196-40-8,51607-77-3,53648-56-9,96243-58-2,124379-08-4,124379-13-1
1,4-anhydro-D-glucitol

: 101069-26-5
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride, ethanol / dimethylformamide / 6 h / Ambient temperature

2: imidazole / dimethylformamide / 3 h / Ambient temperature

With 1H-imidazole; ethanol; acetyl chloride; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90454-3

Reference yield:

: 55730-73-9,86362-57-4
(2S,3R,4S)-2-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-tetrahydro-furan-3,4-diol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 101069-26-5
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 3h; Yield given; Ambient temperature;
DOI:10.1016/S0008-6215(00)90454-3

Reference yield: 98.0%

: 101069-26-5
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

: 101125-99-9
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

Guidance literature:: With dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dimethyl sulfoxide; for 3h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90454-3