1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

Base Information

Chemical Name:1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose
CAS No.:101125-99-9
Molecular Formula:C₂₅H₃₂O₅Si
Molecular Weight:440.612
Hs Code.:

Synonyms:1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

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Chemical Property of 1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

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Technology Process of 1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

There total 4 articles about 1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 101069-26-5
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-glucitol

: 101125-99-9
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

Guidance literature:: With dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dimethyl sulfoxide; for 3h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90454-3

Reference yield:

: 55730-73-9,86362-57-4
(2S,3R,4S)-2-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-tetrahydro-furan-3,4-diol

: 101125-99-9
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 3 h / Ambient temperature

2: 98 percent / 1-ethyl-3-(3'-dimethylaminopropyl)carbodi-imide hydrochloride, dichloroacetic acid / dimethylsulfoxide / 3 h / Ambient temperature

With 1H-imidazole; dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90454-3

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 101125-99-9
1,4-anhydro-2-O-tert-butyldiphenylsilyl-5,6-O-isopropylidene-D-ribo-3-hexulose

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 3 h / Ambient temperature

2: 98 percent / 1-ethyl-3-(3'-dimethylaminopropyl)carbodi-imide hydrochloride, dichloroacetic acid / dimethylsulfoxide / 3 h / Ambient temperature

With 1H-imidazole; dichloro-acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90454-3