N₅-(benzo[d][1,3]dioxol-5-ylmethyl)-N₂,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide

Base Information

• Chemical Name: N₅-(benzo[d][1,3]dioxol-5-ylmethyl)-N₂,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide
• CAS No.: 1198620-31-3
• Molecular Formula: C₃₀H₂₇N₃O₇
• Molecular Weight: 541.56

Synonyms:N₅-(benzo[d][1,3]dioxol-5-ylmethyl)-N₂,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide

Chemical Property of N₅-(benzo[d][1,3]dioxol-5-ylmethyl)-N₂,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide

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Technology Process of N₅-(benzo[d][1,3]dioxol-5-ylmethyl)-N₂,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide

There total 5 articles about N₅-(benzo[d][1,3]dioxol-5-ylmethyl)-N₂,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1,3-benzodioxol-5-ylmethyl amine (2620-50-0) + N,7-bis(benzyloxy)-3-oxo-1,3-dihydrofuro[3,4-c]pyridine-6-carboxamide (1198621-05-4) → N5-(benzo[d][1,3]dioxol-5-ylmethyl)-N2,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide (1198620-31-3)

Guidance literature:

at 70 ℃; for 0.5h;

Reference yield:

N,3-bis(benzyloxy)-4,5-bis(hydroxymethyl)picolinamide (1198621-04-3) → N5-(benzo[d][1,3]dioxol-5-ylmethyl)-N2,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide (1198620-31-3)

Guidance literature:

Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane / 20 °C

2: 0.5 h / 70 °C

With manganese(IV) oxide; In dichloromethane;

Reference yield:

N,9-bis(benzyloxy)-3,3-dimethyl-1,5-dibydro-[1,3]dioxepino[5,6-c]pyridine-8-carboxamide (1198621-03-2) → N5-(benzo[d][1,3]dioxol-5-ylmethyl)-N2,3-bis(benzyloxy)-4-(hydroxymethyl)pyridine-2,5-dicarboxamide (1198620-31-3)

Guidance literature:

Multi-step reaction with 3 steps

1: formic acid / tetrahydrofuran; water / 2 h / 70 °C

2: manganese(IV) oxide / dichloromethane / 20 °C

3: 0.5 h / 70 °C

With manganese(IV) oxide; formic acid; In tetrahydrofuran; dichloromethane; water;

upstream raw materials:

1,3-benzodioxol-5-ylmethyl amine

N,7-bis(benzyloxy)-3-oxo-1,3-dihydrofuro[3,4-c]pyridine-6-carboxamide

N,3-bis(benzyloxy)-4,5-bis(hydroxymethyl)picolinamide

N,9-bis(benzyloxy)-3,3-dimethyl-1,5-dibydro-[1,3]dioxepino[5,6-c]pyridine-8-carboxamide

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