<1R-(1α,2β,3β)>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid

Base Information

• Chemical Name: <1R-(1α,2β,3β)>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid
• CAS No.: 141042-69-5
• Molecular Formula: C₁₅H₁₇NO₄
• Molecular Weight: 275.304

Synonyms:<1R-(1α,2β,3β)>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid

Chemical Property of <1R-(1α,2β,3β)>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid

Chemical Property:

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Technology Process of <1R-(1α,2β,3β)>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid

There total 15 articles about <1R-(1α,2β,3β)>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-(4-morpholinylcarbonyl)-2-formyl-3-phenylcyclopropane (140926-05-2,141042-62-8,141506-51-6,141506-55-0,141506-57-2,141506-58-3) → (1S,2S,3R)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid (130780-73-3,130855-62-8,141042-66-2,141042-69-5,141042-73-1,141042-77-5,141506-33-4,141506-36-7)

Guidance literature:

With jones reagent; In acetone; at 0 ℃; for 2h;

DOI:10.1016/S0040-4039(00)97718-9

Reference yield: 76.0%

<1R-(1α,2β,3α)>-1-(4-morpholinylcarbonyl)-3-phenylcyclopropane-2-carboxaldehyde (141042-62-8) → <1R-(1α,2β,3β)>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid (141042-69-5)

Guidance literature:

With jones' reagent; In acetone; at 0 - 5 ℃; for 2h;

DOI:10.1021/jm00088a005

Reference yield:

((1S,2S,3R)-2-Hydroxymethyl-3-phenyl-cyclopropyl)-morpholin-4-yl-methanone (130780-69-7,141041-95-4,141506-48-1,141506-56-1) → (1S,2S,3S)-2-(Morpholine-4-carbonyl)-3-phenyl-cyclopropanecarboxylic acid (130780-73-3,130855-62-8,141042-66-2,141042-69-5,141042-73-1,141042-77-5,141506-33-4,141506-36-7)

Guidance literature:

With jones reagent; In acetone; at 0 ℃; for 2h; Yield given;

DOI:10.1016/S0040-4039(00)97718-9

upstream raw materials:

((1S,2S,3R)-2-Hydroxymethyl-3-phenyl-cyclopropyl)-morpholin-4-yl-methanone

(Z)-cinnamyl alcohol

endo-6-phenyl-3-oxabicyclo<3.1.0>hexan-2-one

cis-3-phenyl-2-propen-1-yl diazoacetate

Downstream raw materials:

<1R-<1α(1R*,2R*,3S*),2β,5α>>-2-(4-morpholinylcarbonyl)-3-phenylcyclopropanecarboxylic acid (-)-menthol ester

(2S,3R,4S)-2-<carbonyl>-3-(4-thiazoyl)-L-alanyl>amino>-1-cyclohexyl-3,4-dihydroxy-6-methylheptane

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