3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

Base Information

Chemical Name:3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride
CAS No.:118466-46-9
Molecular Formula:C₄₀H₄₀ClNO₁₄
Molecular Weight:794.209
Hs Code.:

Synonyms:3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

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Chemical Property of 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

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Technology Process of 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

There total 5 articles about 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 118466-45-8
3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

: 118466-46-9
3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 2h;

Reference yield:

: 109714-38-7
allyl 2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 118466-46-9
3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / silver trifluoromethanesulphonate, collidine, 4 Angstroem molecular sieves / CH₂Cl₂ / 12 h / Ambient temperature

2: 86 percent / tris(triphenylphosphine)rhodium(I) chloride / ethanol; H₂O / 16 h / Heating

3: 93 percent / mercury(II) oxide, mercury(II) chloride / acetone; H₂O / 5 h

4: 99 percent / DMF, oxalyl chloride / CH₂Cl₂ / 2 h

With 2,3,5-trimethyl-pyridine; oxalyl dichloride; 4 A molecular sieve; silver trifluoromethanesulfonate; N,N-dimethyl-formamide; mercury dichloride; mercury(II) oxide; Wilkinson's catalyst; In ethanol; dichloromethane; water; acetone;

Reference yield:

: 118466-43-6
allyl 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 118466-46-9
3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranosyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / tris(triphenylphosphine)rhodium(I) chloride / ethanol; H₂O / 16 h / Heating

2: 93 percent / mercury(II) oxide, mercury(II) chloride / acetone; H₂O / 5 h

3: 99 percent / DMF, oxalyl chloride / CH₂Cl₂ / 2 h

With oxalyl dichloride; N,N-dimethyl-formamide; mercury dichloride; mercury(II) oxide; Wilkinson's catalyst; In ethanol; dichloromethane; water; acetone;