3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

Base Information

Chemical Name:3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose
CAS No.:118466-45-8
Molecular Formula:C₄₀H₄₁NO₁₅
Molecular Weight:775.763
Hs Code.:

Synonyms:3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

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Chemical Property of 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

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Technology Process of 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

There total 4 articles about 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 118466-44-7,118493-93-9
prop-1-enyl 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 118466-45-8
3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

Guidance literature:: With mercury dichloride; mercury(II) oxide; In water; acetone; for 5h;

Reference yield:

: 109714-38-7
allyl 2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 118466-45-8
3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / silver trifluoromethanesulphonate, collidine, 4 Angstroem molecular sieves / CH₂Cl₂ / 12 h / Ambient temperature

2: 86 percent / tris(triphenylphosphine)rhodium(I) chloride / ethanol; H₂O / 16 h / Heating

3: 93 percent / mercury(II) oxide, mercury(II) chloride / acetone; H₂O / 5 h

With 2,3,5-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; mercury dichloride; mercury(II) oxide; Wilkinson's catalyst; In ethanol; dichloromethane; water; acetone;

Reference yield:

: 118466-43-6
allyl 3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranoside

: 118466-45-8
3-O-(3',4',6'-tri-O-acetyl-2'-deoxy-2'-phthalimido-β-D-glucopyranosyl)-2-O-benzoyl-4-O-benzyl-α-L-rhamnopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / tris(triphenylphosphine)rhodium(I) chloride / ethanol; H₂O / 16 h / Heating

2: 93 percent / mercury(II) oxide, mercury(II) chloride / acetone; H₂O / 5 h

With mercury dichloride; mercury(II) oxide; Wilkinson's catalyst; In ethanol; water; acetone;